Gas sensors measurement setup

A custom setup for measurement of ultra-low electrical currents as low as 1 pA. A furnace is equipped with a silicon tube with 141 cm^3 volume with sapphire sample holder. The sample holder has 2 x 1,5 cm area for samples contcted with a silver paste to gold wire contacts. The atmosphere is chosen by mixing two of four connected pressure bottles in desired ratio. The 100 sccm flow of gas mixture is divided into two branches, one flowing through a bubbler with destilled water, allowing for a measurement in various relative humidities.

Specification

Prometheus Kilns PRO-1 PRG with PID regulator Omron E5CC

Red-y Smart Series (Vögtlin Instruments) flow controller

Keithley 6221 AC and DC current source

Keithley 6487 Picoammeter / Voltage Source

Agillent 34410A with Honeywell HIH-4000 002 humidity sensor

 Keithley 2000 Multimeter with a K-type thermocouple

Notable features

  • Ability to mix two of four connected gas mixtures in ratio of down to 1 : 99.
  • Heating up to 300°C.
  • Measurements at increased relative humidity.
  • Two identical measurement chambers for simultaneous measurements.
  • Sapphire substrate holder with two switchable channels for different samples.

Contact person

Michal Patrnčiak, Mgr.

PhD. Student