Marián Mikula, doc. Ing., PhD.

Researcher, Scientific Research Department

Manager of Detached Department Turany

Contact

Bratislava, Turany
02/602 95 271, 244
E-1111-2019
0000-0001-5643-7023
Show publications

Bio

Researcher and since 2018 associate professor at the Department of Experimental Physics, FMPI CU. Currently an employee of CENAM. Expert in physical deposition technologies and nanostructure design of hard coatings based on TM nitrides and TM diborides. The area of expertise includes structural analysis and mechanical properties of thin films and coatings. In the educational field, he will focus on physical metallurgy and physical methods of preparing thin films.

Specialization research areas

Hard coatings Nanostructured materials Thin ceramic films Transmission electron microscopy Analysis of chemical composition Structure analysis Nitrides X-ray diffraction Scanning electron microscopy Mechanical and tribological properties Oxidation resistance Ball-on-disc Thermal stability Transition metal diborides Nanoindentation

Education

2018

Habilitation thesis: Hard nanostructured coatings

Comenius University in Bratislava, Slovakia, Faculty of Mathematics, Physics and Informatics, Department of Experimental Physics
2007

PhD thesis: Hard and superhard coatings based on titanium 

Institute of Materials and Machine Mechanics, Slovak Academy of Sciences, Slovakia
2002

Diploma thesis: Preparation and properties of wear-resistant ceramic based on B4C

Slovak Technical University, Bratislava, Slovakia, Faculty of Mechanical Engineering, Department of Materials and Technologies

Reviewer activities

Reviewer

Acta Materialia, Scripta Materialia, Materials and Design, Surface and Coatings Technology, Thin Solid Films, Vacuum, Journal of Alloys, and Compounds

Elsevier, The Netherlands
Reviewer

Journal of Vacuum Science and Technology A

American Institute of Physics (AIP), USA

Other activities

Member

Society for New Materials and Technologies

Slovak Republic
Member

Slovak Silicate Society

Slovak Republic
Member

Scientific Council in Institute of Materials and Machine Mechanics

Slovak Academy of Sciences, Slovak Republic

Awards

2017

Great Researcher Award – Institute of Materials and Machine Mechanics

Slovak Academy of Sciences, Slovak Republic

Projects

National

Hard coatingsSuperconductivitySensorsBiomaterials
Leader

Central European Platform for Plasma-Enabled Surface Engineering, HORIZON-WIDERA-2023-ACCESS-04-01

Horizon Europe
Hard coatings
Key Researcher

Ultra-high temperature thin coatings for aerospace industry. Contract No.: 4000136772/21/NL/SC/hm

European Space Agency (ESA)
Hard coatings
Key Researcher

Potential solid lubricant for extreme temperatures based on vanadium boride. Contract No.: 4000132355/20/NL/SC

European Space Agency (ESA)
Hard coatings
Key Researcher

Development of nanostructured coatings with an inactivating effect on viruses and bacteria for different types of flexible materials.; No. NFP313010AUH4;

Operational program Integrated infrastructure ERDF
Hard coatings
Principal Investigator

APVV-21-0042: Hard and tough boride- and nitride-based coatings prepared by advanced PVD techniques.

Slovak Research and Development Agency (APVV)
Hard coatings
Researcher

VEGA 1/0473/24: Theoretical study and experimental preparation of multilayers based on transition metal diborides with enhanced fracture toughness

VEGA
Hard coatings
Researcher

VEGA 1/0296/22: Transition-metal diborides-based hard films prepared by advanced PVD methods

VEGA

Teaching activities

Courses taught

Course Objectives

In the first part, the student will gain knowledge in the field of phase transformations in technical materials. They will get acquainted with the formation of solid solutions, with nucleation and conditions of intergrain interfaces and their influence on the shape of crystals, with their temperature stability, with the influence of point defects on the structure of solid solutions. He will also gain knowledge about solidification of alloys, diffusion and non-diffusion transformations, shape memory and decomposition mechanisms, precipitation. In the second part, they will get acquainted with the conditions of deformation behavior of alloys, with the influence of dislocations and surface defects on the strengthening of materials. The student will understand the concept of nanostructured materials from the point of view of mechanical behavior and will also gain a comprehensive idea of fracture mechanics, material creep and material fatigue.

Syllabus

Point defects in lattices, solid solutions, nucleation, surface strains, Wulff shape. Phase transitions in solid solutions. Solidification, dendrites. Peritectic, monotectic, eutectic, eutectoid transformations. TTT diagrams, martensitic transformation. Intermediate phases. Steels, alloying. Precipitation, spinodal decomposition in alloys, phase segregation. Dislocation mechanisms. Deformation mechanisms, strengthening. Tensile test. Stacking faults, Grain boundaries. Fracture mechanics, creep, material fatigue.

Prerequisite Courses

Structure and mechanical properties of solids (2-FTL-107/15)

Course Objectives

The student will first get acquainted with the technical possibilities of achieving vacuum, its measurement and control of working gases. He will gain a comprehensive knowledge of physical methods of preparation of thin films (evaporation, sputtering, arc evaporation, pulsed laser deposition), where he will be explained in detail the physical aspects of the processes. The student will gain information about the growth of thin films, the influence of deposition parameters on the structure and properties of films. In the last part he will be introduced to the possibilities of creating functional structures in films using ion treatment and lithographic methods.

Syllabus

vacuum pumps, scales and flow controllers, Langmuir probe, mass spectroscopy, evaporation, DC and RF sputtering, magnetron, glow discharge, plasma parameters, high energy pulses (HiPPMS), pulsed laser deposition, laser optics, ablation mechanism, arc evaporation, cathode macroparticle filtering, thin film growth, surface energy, thermodynamic nucleation model, zonal models, texture, epitaxy, focused ion beam, nanotubes, electron lithography, optical lithography

Course Objectives

The student will gain knowledge in the field of preparation, structure, and properties of technical materials. In the introductory part of the course, they will get acquainted with amorphous/crystalline materials, with point defects in materials, dislocations and surface defects, their influence on mechanical properties. It will also focus on phase transformations in solid solutions, steels, and non-ferrous alloys, on heat treatment methods and its influence on mechanical properties. The student will get a comprehensive idea of material fatigue, of material creep. They will also learn basic information about structural ceramics and thin ceramic films and how to prepare them and their properties.

Syllabus

Basic construction of materials, defects in lattices, dislocation mechanisms. Deformation mechanisms, strengthening. Tensile test, Surface defects, Grain boundaries. Solid solutions, Phase transformations in solid solutions. Steels, and their alloying. Peritectic, monotectic, eutectic, eutectoid transformations. IRA, ARA diagrams, martensitic transformation. Precipitation, spinodal decomposition in Al alloys. Structural ceramics – oxides, carbides, borides, powder metallurgy, thin films, creep, fracture mechanics, material fatigue.

Students supervision

Supervisor of bachelors, master, and PhD. students.